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Environmentally benign silver bio-nanomaterials as potent antioxidant, antibacterial, and antidiabetic agents: Green synthesis using Salacia oblonga root extract

Authors: Guru Kumar Dugganaboyana,Chethan Kumar Mukunda,Anisha Jain,Raghavendra Mandya Kantharaju,Rani R. Nithya,Divya Ninganna,Rathi Muthaiyan Ahalliya,Ali A. Shati,Mohammad Y. Alfaifi,Serag Eldin I. Elbehairi,Ekaterina Silina,Victor Stupin,Gopalakrishnan Velliyur Kanniappan,Raghu Ram Achar,Chandan Shivamallu,Shiva Prasad Kollur
Journal: Frontiers in Chemistry
Publisher: Frontiers Media SA
Publish date: 2023-2-3
ISSN: 2296-2646 DOI: 10.3389/fchem.2023.1114109
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It has been brought to light by a reader that Figure 4 (FT-IR spectrum) in this article appears to be identical to Figure 5 published by a largely overlapping author group (Kumar et al., 2023, https://doi.org/10.1186/s12906-023-03982-1). In that paper, the spectrum is presented as data from silver nanoparticles synthesized using Viscum orientale leaf extract, while here it is claimed to be from nanoparticles synthesized using Salacia oblonga root extract. The duplication of what is purported to be unique spectroscopic data from two entirely different biological sources is a serious breach of research ethics and irreparably damages the credibility of both publications.

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2 weeks, 5 days ago

Here are both Figures in two difference publications.

2 weeks, 5 days ago

Upon inspection of this paper in light of that concern, another critical error has been identified.

The paper reports two different sizes for the same batch of SOR-AgNPs using two different techniques, and the values are off by a factor of more than 3, with no explanation provided. This is a major inconsistency that invalidates the core characterization of the material.

– Statement in Results (Page 4, Section 3.3: Analysis using a scanning electron microscope (SEM)):

“SEM analysis of the morphology (viz size and shape) of SOR-AgNPs showed multiform nanoparticles… average size range of between 59 and 78 nm.”

– Statement in Results (Page 5, Section 3.9: Dynamic light scattering (DLS) measurement):

“The diameter of SOR-AgNPs is 181.5 nm, according to the size distribution histogram of DLS (Figure 7).”

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